R. Oldenbourg Verlag: Zeitschrift für Kristallographie

Volume 213 · Issue 4 · 1998
Zeitschrift für Kristallographie - New Crystal Structures
International journal for structural, physical, and chemical aspects of crystalline materials
Language of publication: English
Volume 213: 4 issues appear in 1998
ISSN: 1433-7266

Rubrik: Inorganic Crystal Structures

H. G. von Schnering, J. Llanos, Yu. Grin, W. Carrillo-Cabrera, E.-M. Peters, K. Peters and R. Nesper
Crystal structure of dicaesium disodium tetragermanide(4-), Cs₂Na₂Ge₄, p. 661
NCS 409262

R. Kröner, K. Peters, H. G. von Schnering and R. Nesper
Crystal structure of dibarium tetragermanide(4-), Ba₂Ge₄, p. 662
NCS 409260

R. Kröner, K. Peters and H. G. von Schnering
Crystal structure of barium tristannide, BaSn₃, p. 663
NCS 409263

R. Kröner, K. Peters, H. G. von Schnering and R. Nesper
Crystal structure of the clathrate-II, Ba₁₆Ga₃₂Sn₁₀₄, p. 664
NCS 409264

H. G. von Schnering, R. Kröner, W. Carrillo-Cabrera, K. Peters and R. Nesper
Crystal structure of the novel chiral clathrate, Ba₆In₄Ge₂₁, p. 665
NCS 409266

R. Kröner, K. Peters, H. G. von Schnering and R. Nesper
Crystal structure of the clathrates K₈Ga₈Si₃₈ and K₈Ga₈Sn₃₈, p. 667
NCS 409247 409248

R. Kröner, K. Peters, H. G. von Schnering and R. Nesper
Crystal structure of the clathrates Rb₈Al₈Ge₈ and Rb₈Al₈Sn₃₈, p. 669
NCS 409249 409250

R. Kröner, K. Peters, H. G. von Schnering and R. Nesper
Crystal structure of the clathrates Cs₈Ga₈Ge₃₈ and Cs₈Ga₈Sn₃₈, p. 671
NCS 409251 409252

H. G. von Schnering, H. Menke, R. Kröner, E.-M. Peters, K. Peters and R. Nesper
Crystal structure of the clathrates Rb₈In₈Ge₃₈ and K₈In₈Ge₃₈, p. 673
NCS 409253 409254

R. Kröner, K. Peters, H. G. von Schnering and R. Nesper
Crystal structure of the clathrates K₈Al₈Ge₃₈ and K₈Al₈Sn₃₈, p. 675
NCS 409255 409256

H. G. von Schnering, R. Kröner, H. Menke, K. Peters and R. Nesper
Crystal structure of the clathrates Rb₈Ga₈Sn₃₈, Rb₈Ga₈Ge₃₈ and Rb₈Ga₈Si₃₈, p. 677
NCS 409257 409258 409259

H. G. von Schnering, W. Carrillo-Cabrera, R. Kröner, E.-M. Peters, K. Peters and R. Nesper
Crystal structure of the clathrate b-Ba₈Ga₁₆Sn₃₀, p. 679
NCS 409265

Y.-Q. Zheng, J. Nuss and H. G. von Schnering
Crystal structure of dicopper(I) octa-m₃-chlorohexachloro-octahedro-hexatungstate(2-), Cu₂[(W₆Cl)Cl], p. 680
NCS 409272

Y.-Q. Zheng, K. Peters and H. G. von Schnering
Crystal structure of dithallium(I) octa-m₃-bromohexabromo-octahedro-hexatungstate(2-), Tl₂[(W₆Br)Br], p. 681
NCS 409273

M. Somer, W. Carrillo-Cabrera, K. Peters and H. G. von Schnering
Crystal structure of tetrasodium octastrontium catena-[octaphosphido(3-)]-
[diphosphido(4-)]tetraaluminate(III) [diphosphide(4-)], Na₄Sr₈[Al₄P₈(P₂)][P₂], p. 683
NCS 409319

M. Somer, W. Carrillo-Cabrera, K. Peters and H. G. von Schnering
Crystal structure of tetrasodium octaeuropium(II) [octaphosphido(3-)]-
bis[diphosphido(4-)]tetraaluminate(III), Na₄Eu₈[Al₄P₈(P₂)₂], p. 685
NCS 409320

M. Somer, W. Carrillo-Cabrera, K. Peters, E.-M. Peters and H. G. von Schnering
Crystal structure of tetrasodium octaeuropium(II) pentaphosphido(3-)-diphosphido(4-)-digallate(III) catena-triphosphido(3-)-diphosphido(4-)-digallate(III), Na₄Eu₈[Ga₂P₅(P₂)][GaP₃(P₂)], p. 687
NCS 409321

U. Bolle, W. Carrillo-Cabrera, K. Peters and H. G. von Schnering
Crystal structure of tetrastrontium dilithium hexasilicide(10-), Sr₄Li₂Si₆, p. 689
NCS 409295

S. Masselmann and G. Meyer
Crystal structure of barium heptachloroeuropate(III), Ba₂[EuCl₇], p. 690
NCS 408502

M. Heuer, K. Bente, M. Steins and A. Rothkopf
Crystal structure of calcium tectozincotrisilicate, CaZnSi₃O₈, p. 691
NCS 409286

K. O. Klepp and D. Sturmayr
Crystal structure of kalium copper trithiohafnate(IV), KCuHfS₃, p. 693
NCS 409293

K. O. Klepp and A. Kolb
Crystal structure of dicaesium triselenozirconate(IV), Cs₂ZrSe₃, p. 694
NCS 409294

U. Eggenweiler, E. Keller, V. Krämer, C. A. Meyer and J. Ketterer
Crystal structure of tribismuth tetraoxide chloride, Bi₃O₄Cl, p. 695
NCS 409330

D. Königstein and M. Jansen
Crystal structure of strontium dihydrogenphosphate, Sr(H₂PO₄)₂, p. 696
NCS 408339

Rubrik: Organic and Metalorganic Crystal Structures

B. Becker, J. Chojnacki, A. Konitz and W. Wojnowski
Crystal structure of bis(triphenylphosphine)[O,O,O-tris(1,1-dimethyl-ethyl)monothioorthosilicato-S]silver, C₄₈H₅₇AgO₃P₂SSi, p. 697
NCS 409287

J.-M. Delafontaine, R. Julien, B. Legendre, A. Mazurier and A. Tomas
Crystal structure of 4-azaoctane-1,8-diammonium hexachloroplatinate(IV) hydrogenchloride solvate, [C₇H₂₁N₃]PtCl₆ · HCl, p. 699
NCS 409234

K. Peters, E.-M. Peters, R. Reinhardt and H. Quast
Crystal structure of cis-N,N´-bis(1-methyl-3-phenyl-1-propen-3-onyl)-1,2-cyclopropanediamine, C₃H₆N₂(C₁₀H₉O)₂, p. 701
NCS 409244

K. Peters, E.-M. Peters, R. Reinhardt and H. Quast
Crystal structure of 1,4,8,11-tetraaza-5,7,12,14-tetramethylcyclotetradeca-4,6,11,13-tetraene bis(hydroperchlorate), (C₇H₁₂N₂)₂(HClO₄)₂, p. 703
NCS 409245

K. Peters, E.-M. Peters, D. Regnat and H. Quast
Crystal structure of 1,4,9,9-tetramethyl-6-phenyl-1,2,3,4,6,7,8-heptaaza-spiro[4.4]nona-2,7-diene, C₁₂H₁₇N₇, p. 705
NCS 56495

K. Peters, E.-M. Peters, M. L. Werner and H. Quast
Crystal structure of (1S*,7R*,10S*,16R*)-2,6,11,15-tetraaza-tricyclo[14.2.0.0^7,10]octadeca-2,4,11,13-tetraene bis(hydroperchlorate), (C₇H₁₀N₂)₂(HClO₄)₂, p. 707
NCS 409275

K. Peters, E.-M. Peters, M. Ach and H. Quast
Crystal structure of N-methyl-N-(2-methylpropanoyl)-2-(N-methylamino)aniline, (C₆H₄NHCH₃)N(CH₃)(COC₃H₇), p. 709
NCS 409283

K. Peters, E.-M. Peters, M. Ach and H. Quast
Crystal structure of 3,4-dihydro-2,2,4-trimethyl-3-(N-phenylimino)-2H-1,4-benzoxazine, (CH₃)₃(NC₆H₅)C₈H₄NO, p. 711
NCS 409284

K. Peters, E.-M. Peters, T. Dietz and H. Quast
Crystal structure of 1,5-dimethylbicyclo[3.3.0]octa-2,6-diene palladium dichloride, C₁₀H₁₄PdCl₂, p. 713
NCS 409296

K. Peters, E.-M. Peters, M. Witzel and H. Quast
Crystal structure of 3-(phenylethinyl)-2-oxatricyclo[3.3.1.1^5,7]decan-1-ol, C₉H₁₂O(OH)(C₂C₆H₅), p. 715
NCS 409297

K. Peters, E.-M. Peters, U. M. Doht and H. Quast
Crystal structures of the diastereomeric 2-chloro-3-methyl-1-(2-methyl-phenyl)-1-phenyl-1-butenes, C₄H₄(C₆H₅)(C₇H₇)ClCH₃, p. 717
NCS 409299

K. Peters, E.-M. Peters, U. M. Doht and H. Quast
Crystal structures of the diastereomeric 2-bromo-3-methyl-1-(2-methylphenyl)-1-phenyl-1-butenes, C₄H₄(C₆H₅)(C₇H₇)BrCH₃, p. 720
NCS 409300 409301

K. Peters, E.-M. Peters, J. Balthasar and H. Quast
Crystal structure of 2,4,6-tri-tert-butylphenylazide, (C₄H₉)₃C₆H₂N₃, p. 723
NCS 409274

P. Lemoine, B. Viossat and D. Nguyen-Huy
Crystal structure of cis-dichloro(metforminuro)gold(III) dimethylacetamide, C₁₆H₃₈Au₂Cl₄N₁₂O₂, p. 726
NCS 409127

M. Shoja, M.-W. Yen and L. Peterson
Crystal structure of 6-hydroxyflavone, C₁₅H₁₀O₃, p. 729
NCS 409276

M. Shoja
Crystal structure of 3-hydroxy-6-methoxyflavone, C₁₆H₁₂O₄, p. 731
NCS 409302

J. Zukerman-Schpector, A. Helio Stefani, C. I. Valduga, C. A. Brandt and I. Caracelli
Crystal structure of 5-(iodomethyl)-3-(5-iodo-7-oxabicyclo[4.3.0]non-8-ylidene)oxolan-2-one, C₁₃H₁₆I₂O₃, p. 733
NCS 409277

J. Zukerman-Schpector, C. C. Carvalho, H. M. C. Ferraz, F. L. C. Pereira, L. B. Zinner and G. Vicentini
Crystal structure of 1-benzyl-2-methyl-3-carbethoxy-7S-iodo-4,5,6,7-3a(R),7a(S)-hexahydroindole, C₁₉H₂₄INO₂, p. 735
NCS 409303

W. Frey, A. Lieberknecht, H. Griesser, R. D. Bravo, P. A. Colinas and R. J. Grigera
Crystal structure of (2S,4R,5R,6R)-2-(4,5-dibenzyloxy-6-benzyloxymethyl tetrahydropyranyl)triphenylphosphonium tetrafluoroborate, a-C₄₅H₄₄PBF₄O₄ and of (2R,4R,5R,6R)-2-(4,5-dibenzyloxy-6-benzyloxymethyl tetrahydropyranyl)triphenylphosphonium tetrafluoroborate,b-C₄₅H₄₄PBF₄O₄, p. 737
NCS 409279

B. Barbier, H. Euler, A. Kirfel, S. Schüren and H. Wamhoff
Crystal structure of 2-benzyl-3-phenyl-5-phenylimino-D³-1,2,4-thia-diazoline, C₂₁H₁₇N₃S, p. 741
NCS 409280

S. Aldoshin, I. Chuev, O. Filipenko, V. Lokshin, R. Guglielmetti and G. Pèpe
Crystal structure of 8-methyl-8-phenyl-[8H]-pyrano[3,2-f]quinoline, C₁₉H₁₅NO, p. 743
NCS 409285

K. Peters, E.-M. Peters, N. A. Braun, M. A. Ciufolini
Crystal structure of 1-[(1´S)-1´-benzyl-2´-(4-bromobenzoyloxy)ethyl]-1-azaspiro[4.5]deca-6,9-dien-2,8-dione hydrate, C₂₅H₂₂NO₄Br · H₂O, p. 745
NCS 409246

K. Peters, E.-M. Peters, L. Kirmaier and M. Weidenbruch
Crystal structure of 1,1,2,2-tetra-tert-butyl-1,2-dichlorodisilane, [(C₄H₉)₂ClSi]₂, p. 747
NCS 409269

K. Peters, E.-M. Peters, G. Seufert and V. Jäger
Crystal structure of 3-[2´-(1´´,3´´-dioxolane-2´´-yl)-1´-nitroethyl]cyclohexanone, [(C₆H₉O)(C₃H₅O₂)]C₂H₃NO₂, p. 749
NCS 409270

K. Peters, E.-M. Peters, J. Raczko and V. Jäger
Crystal structure of (2R,3S,1´S)-3,5-O-benzylidene-1-nitro-2,3,5-pentanetriol, (C₆H₅)C₄H₆O₂(C₂H₄NO₃), p. 751
NCS 409288

K. Peters, E.-M. Peters, J. Raczko and V. Jäger
Crystal structure of (3S,4S,5R,1´S)-1,3-O-benzylidene-6-methyl-4-nitro-1,3,5-heptanetriol, (C₆H₅)C₄H₆O₂(C₅H₁₀NO₃), p. 753
NCS 409290

K. Peters, E.-M. Peters, J. Raczko and V. Jäger
Crystal structure of (3S,4R,5R,1´S)-1,3-O-benzylidene-6-methyl-4-nitro-1,3,5-heptanetriol, (C₆H₅)C₄H₆O₂(C₅H₁₀NO₃), p. 755
NCS 409291

K. Peters, E.-M. Peters, M. Oelgemöller and A. G. Griesbeck
Crystal structure of 4b-hydroxy-4b,6,8,9-tetrahydro-5H-7-thia-9a-aza-benzo[a]azulen-10-one, C₁₂H₁₃NO₂S, p. 757
NCS 409289

K. Peters, E.-M. Peters, T. Irrgang and A. Hetzheim
Crystal structure of 2,4-dimethyl-5-4´-methylphenyl-7-pyrid-3-ylmethyl-aminoimidazo[1,5-b]pyridazine, (C₇H₇)C₈H₇N₃(C₆H₇N₂), p. 759
NCS 409307

K. Peters, E.-M. Peters, K. Grunwald and A. Hetzheim
Crystal structure of 2-amino-3-phenacyl-4,5-dimethyloxazolium bromide, [C₃NO]⁺(NH₂)(CH₃)₂[(CH₂CO)C₆H₅]Br^-, p. 761
NCS 409310

K. Peters, E.-M. Peters, B. Schoknecht and A. Hetzheim
Crystal structure of 2,4-dimethyl-5-4´-methoxyphenyl-7-thioxoimidazo-[1,5-b]pyridazine, C₆H₂N₃S(CH₃)₂C₆H₄OCH₃, p. 763
NCS 409311

K. Peters, E.-M. Peters, J. Hegmann and M. Christl
Crystal structure of [1R*,2S*,3R*(S*),4S*]-a-oxo-3-(10-oxo-9-phenyl-bicyclo[6.2.0]-
dec-1(8)-en-9-ylbicyclo[2.2.1]heptane-2-acetic acid methyl ester, C₄O(C₆H₁₂)(C₆H₅)[C₇H₁₀(C₃H₃O₃)], p. 765
NCS 409308

K. Peters, E.-M. Peters, G. Hüttner and M. Christl
Crystal structure of 5,6-dihydro-2-oxo-3-phenyl-2H-oxocin-8-carboxylic acid methyl ester, C₇H₆O₂(C₆H₅)C₂H₃O₂, p. 767
NCS 409309

K. Peters, E.-M. Peters, E. Feineis and M. Christl
Crystal structure of 6-diethylamino-1,4-dihydro-5-methyl-4-oxo-3-phenyl-1-(4-toluoyl)pyridazine, C₄N₂O(CH₃)(COC₆H₄CH₃)(N(C₂H₅)₂)(C₆H₅), p. 769
NCS 409312

S. A. Warda
Crystal structure of dimeric aqua(N-salicylidene-rac-alaninato)copper(II) monohydrate, C₁₀H₁₁CuNO₄ · H₂O, p. 771
NCS 409833

A. Pilz, U. Müller, I. Díaz and V. Fernández
Crystal structure of 2-amino-5-methyl-3H-1,3,4-thiadiazolium chloride hydrate, [C₂N₂SH(CH₃)(NH₂)]⁺Cl^- · H₂O, p. 773
NCS 409304

G. Frenzen, A. Pilz, H. Frauenrath and S. Reim
Crystal structure of dibromo[(-)-2,2-dimethyl-4,5-bis(diphenylphoshinomethyl)-1,3-dioxolane-P,P´] nickel-dichloromethane (1/1), C₃₁H₃₂Br₂NiO₂P₂ · CH₂Cl₂, p. 775
NCS 409305

G. Frenzen, S. Rabe, H. Frauenrath and S. Reim
Crystal structure of diiodo[(-)-2,2-dimethyl-4,5-bis(diphenylphoshinomethyl)-1,3-dioxolane-P,P´] nickel, C₃₁H₃₂I₂NiO₂P₂, p. 777
NCS 409306

C. Bavoux and M. Perrin, D. P. Lovett, M. A. Ciufoloni
Crystal structure of 9,9a-dihydro-8-methoxy-6-methyl-2-oxo-1H-pyrrolo-(1,2-a)indole, C₁₃H₁₅O₂N, p. 779
NCS 409333

R. Hauptmann, J. Schneider, M. Köckerling and G. Henkel
Crystal structure of tetraphenylphosphonium-2,6-bis(trimethylsilyl)thiophenolate-toluene (1/0.5), [Ph₄P][SC₆H₃(SiMe₃)₂] · 0.5C₇H₈, p. 781
NCS 409316

R. Hauptmann, J. Schneider and G. Henkel
Crystal structure of ditetrahydrofuranecobalt(II) 2,6-bis(trimethylsilyl)thiophenolate, C₃₂H₅₈O₂Si₄S₂Co, p. 783
NCS 409318

W. Krämer, E. Geyer and D. Schollmeyer
Crystal structure of 1,2-dihydroxytricyclo[5.3.1.1^2,6]dodeca-4,8-dien-3,10,11,12-tetraone, C₂₀H₂₄O₆, p. 785
NCS 409314

W. Krämer, E. Geyer and D. Schollmeyer
Crystal structure of 1,7-dihydroxytricyclo[5.3.1.1^2,6]dodeca-4,9-dien-3,8,11,12-tetraone, C₂₀H₂₄O₆, p. 787
NCS 409315

R. Kempe, A. Spannenberg, P. Kosse, N. Peulecke and U. Rosenthal
Crystal structure of 2,2-bis(h⁵-2,4-cyclopentadiene-1-yl)-2,5-bis(dimethylsilyl)-3,4-bis(phenyl)zirconacyclopentadiene, C₃₀H₃₄Si₂Zr, p. 789
NCS 409322

R. Kempe, A. Spannenberg, C. Lefeber, T. Zippel and U. Rosenthal
Crystal structure of 1-phenyl-2,2-bis(h⁵-2,4-cyclopentadiene-1-yl)-2-pyridine-2-zircona-3-phenyl-3-methylaziridine, C₃₂H₃₅N₂Zr, p. 791
NCS 409323

R. Kempe, A. Spannenberg, N. Peulecke and U. Rosenthal
Crystal structure of dimeric 2,2-bis(h⁵-2,4-cyclopentadiene-1-yl)-2-zirconium-3-trimethylsilyl-4-dimethylsilyl-furan-5-one, C₁₈H₂₆O₂Si₂Zr, p. 793
NCS 409324

S. Henkel, A. Menzel and V. Jäger
Crystal structure of methyl N,O-diacetyl-a-L-acosaminide, C₁₁H₁₉NO₅, p. 795
NCS 409292

H. Irngartinger, A. Altreuther, A. Krebs and F. Toda
Crystal structure of N-methyl-N-phenyl-(2-methyl-3-phenylcyclopropenylidene)ammonium perchlorate, C₁₇H₁₆N⁺ClO₄^-and of 3-cyano-1,2,3-triphenylcycloprop-1-ene-benzene (1/2), C₂₂H₁₅N · 2C₆H₆, p. 797
NCS 409282 409281

Author Index
Formulae Index
Further details of the structure determination can be accessed at the relevant database or ordered from the Fachinformationszentrum Karlsruhe, D-76344 Eggenstein-Leopoldshafen, Germany. To recall the data refer to the CSD-number which is printed in the heading of the article.

[ New Crystal Structures ]